|Publication Year: 2016|
Highlight ID: 658
|Catalytic Pulping of Wood|
The kraft pulping process has been around for more than 100 years. It is cost effective and efficient but provides a low fiber yield and a complex and expensive chemical recovery process. Using oxygen ...
Highlight ID: 659
|Heat Treatment of Green Wood Accomplishes Crystal Hardening|
After centuries of study, the structure of the woody cell wall remains poorly understood. Regarding cellulose crystals in green wood, X-ray methods demonstrate the repeating structure of a crystal, bu ...
Highlight ID: 653
|Improving the Hydrolysis and Fibrillation of Wood Into Cellulose Nanomaterials|
Cellulose nanomaterials have been receiving an increasing amount of interest from both the scientific and industrial communities because of their interesting properties, including good strength, absor ...
|Publication Year: 2015|
Highlight ID: 602
|Cellulose Nanocrystals Chemically Entrap Biocide in Wood|
Forest Service scientists evaluated naturally occurring cellulose nanocrystals (CNC) that are reported to have unique chemical properties and impart high strength were evaluated for the potential to i ...
Highlight ID: 618
|How Does Wood Decay Start?|
How do fungi rot wood? Using new tools, fluorescent dye attached to tiny beads, and laser confocal microscopy, Forest Service scientists were able to follow oxidation on a microscopic level. The infor ...
Highlight ID: 619
|Using Raman Spectroscopy to Analyze Wood, Cellulose-Nanomaterials, and Their Composites|
Raman spectroscopy provides information based on molecular vibrations and is well-suited to analyze wood and cellulose-nanomaterials. Using a recently developed method to determine the fraction of cel ...
|Publication Year: 2013|
Highlight ID: 444
|New Method Measures Localized Stiffness of Thin Paper Materials with a Single Test|
Forest Products Laboratory researchers have developed a method to measure localized stiffness of thin paper materials with a single test. Although developed for use on problems in the paper industry, ...
Highlight ID: 448
|Scientists Determine Critical Factors that Caused Peroxide Explosion in Paper Mill|
In 2001, a peroxide bleach stage at a paper mill in Evadale, Texas, exploded, rupturing two bleaching towers, destroying a pump, and propelling fragments over 800 yards in all directions. There were n ...
|Publication Year: 2012|
Highlight ID: 22
|Forest Service Continues To Make a Better Postage Stamp|
Latest research reduces the environmental effect of stamp materials ...
Highlight ID: 14
|New Cellulose Nanomaterials Pilot Plant Keeps Up With Market Demand|
Materials are being supplied to three government agencies and six partner universities to accelerate the development of advanced cellulose-reinforced composites, and printed, flexible electronic circu ...
Highlight ID: 3
|New SPORL Process Efficiently Converts Biomass to Sugars and Ferment|
Preliminary laboratory evaluation confirms the high performance of the SPORL process for pretreatment of Douglas fir ...
|Publication Year: 2011|
Highlight ID: 283
|High Performance nano-Cellulose Composites|
Cellulose nano-crystals (CNC) and cellulose nano-fibrils (CNF) provide strength properties equivalent to Kevlar and can be used in optically clear applications like composite windshields. The Forest ...
|Publication Year: 2010|
Highlight ID: 175
|Scale-up of cellulose nano material production|
There is considerable research internationally on cellulose nano-materials as reinforcement fibers for high strength composites. A persistent problem has been unavailability of cellulose nano-crystals ...
Agarwal, Umesh P.
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Considine, John M.
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|Materials Research Engineer||608-231-9525|
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Houtman, Carl J.
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|Program Support Assistant||608-231-9465|
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|Physical Science Technician||608-231-9404|
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Scott, C Tim
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|General Engineer (Volunteer)||608-231-9435|
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|Engineering Technician (Materials)||608-231-9405|
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|Research General Engineer||608-231-9520|
|Below are the 50 most recent products author or co-authored by researchers of this unit that have been posted, sorted by publication year and title. To access the complete repository of FPL products, click here.|
|Publication Year||Title||Date Posted|
|2018||Current characterization methods for cellulose nanomaterials||08/09/18|
|2018||Determination of constitutive properties in inverse problem using airy stress function||09/27/18|
|2018||Effect of freeze-drying on the morphology of dried cellulose nanocrystals (CNCs) and tensile properties of poly(lactic) acid-CNC composites||08/27/18|
|2018||Facile synthesis of highly hydrophobic cellulose nanoparticles through post-esterification microfluidization||09/14/18|
|2018||Fungal lignin peroxidase does not produce the veratryl alcohol cation radical as a diffusible ligninolytic oxidant||07/26/18|
|2018||Lessons learned from 150 years of pulping wood||07/26/18|
|2018||Lignin-containing cellulose nanofibril-reinforced polyvinyl alcohol hydrogels||08/08/18|
|2018||Mechanical characterization of cellulose nanofibril materials made by additive manufacturing||10/02/18|
|2018||New cellulose crystallinity estimation method that differentiates between organized and crystalline phases||08/08/18|
|2018||Performance of high lignin content cellulose nanocrystals in poly(lactic acid)||05/30/18|
|2018||Processing bulk natural wood into a high-performance structural material||03/29/18|
|2018||The nanostructures of native celluloses, their transformations upon isolation, and their implications for production of nanocelluloses||04/03/18|
|2017||Cellulosic ethanol byproducts as a bulking agent||06/28/17|
|2017||Chapter 20: Stiffness heterogeneity of multiply paperboard examined with VFM||12/29/16|
|2017||Characterization of extractives in durable and non-durable hardwoods: Black locust, Catalpa, and Honey mesquite||12/13/17|
|2017||Chemical modification of nanocellulose with canola oil fatty acid methyl ester||09/05/17|
|2017||Comparative characterization of extractives in Alaskan Yellow, Eastern Red, and Western Red Cedars||12/13/17|
|2017||Comparative study of fungal deterioration in Liquidambar orientalis mill heartwood extractives||10/05/17|
|2017||Contribution of residual proteins to the thermomechanical performance of cellulosic nanofibrils isolated from green macroalgae||04/03/18|
|2017||Conversion economics of forest biomaterials: risk and financial analysis of CNC manufacturing||10/06/17|
|2017||Effect of sample moisture content on XRD-estimated cellulose crystallinity index and crystallite size||06/28/17|
|2017||Increasing the revenue from lignocellulosic biomass: maximizing feedstock utilization||07/12/18|
|2017||Integrated production of furfural and levulinic acid from corncob in a one-pot batch reaction incorporating distillation using step temperature profiling||07/17/18|
|2017||Integrated production of lignin containing cellulose nanocrystals (LCNC) and nanofibrils (LCNF) using an easily recyclable di-carboxylic acid||09/01/17|
|2017||Low-temperature microbial and direct conversion of lignocellulosic biomass to electricity: advances and challenges||07/24/18|
|2017||Nanocomposites from lignin-containing cellulose nanocrystals and poly(lactic acid)||09/13/17|
|2017||Nanofibrillated cellulose from appalachian hardwoods logging residues as template for antimicrobial copper||08/30/17|
|2017||Phosphomolybdic acid and ferric iron as efficient electron mediators for coupling biomass pretreatment to produce bioethanol and electricity generation from wheat straw||04/14/17|
|2017||Polyoxometalate-mediated lignin oxidation for efficient enzymatic production of sugars and generation of electricity from lignocellulosic biomass||07/27/18|
|2017||Preparation and characterization of the nanocomposites from chemically modified nanocellulose and poly(lactic acid)||04/09/18|
|2017||Producing wood-based nanomaterials by rapid fractionation of wood at 80 °C using a recyclable acid hydrotrope||09/01/17|
|2017||Production of Cellulose Nanocrystals from Raw Wood Via Hydrothermal treatment *||12/20/17|
|2017||Raman spectroscopy in the analysis of cellulose nanomaterials||12/13/17|
|2017||Raman spectroscopy of CNC-and CNF-based nanocomposites||06/07/17|
|2017||Rapid and near-complete dissolution of wood lignin at ≤80°C by a recyclable acid hydrotrope||09/27/17|
|2017||Rheometry of coarse biomass at high temperature and pressure||10/06/17|
|2017||Sensitivity analysis of hybrid thermoelastic techniques||10/06/17|
|2017||Smoothly varying in-plane stiffness heterogeneity evaluated under uniaxial tensile stress||09/27/17|
|2017||Tailored and integrated production of carboxylated cellulose nanocrystals (CNC) with nanofibrils (CNF) through maleic acid hydrolysis||04/26/17|
|2017||Thermally stable cellulose nanocrystals toward high-performance 2D and 3D nanostructures||02/13/18|
|2017||Using a fully recyclable dicarboxylic acid for producing dispersible and thermally stable cellulose nanomaterials from different cellulosic sources||08/25/17|
|2016||A comparison of cellulose nanofibrils produced from Cladophora glomerata algae and bleached eucalyptus pulp||10/07/16|
|2016||A survey of bioenergy research in Forest Service Research and Development||06/09/16|
|2016||Acridine Orange Indicates Early Oxidation of Wood Cell Walls by Fungi||09/07/16|
|2016||Batch fermentation options for high titer bioethanol production from a SPORL pretreated Douglas-Fir forest residue without detoxification||12/06/16|
|2016||Bioconversion of woody biomass to biofuel and lignin co-product using sulfite pretreatment to overcome the recalcitrance of lignocelluloses (SPORL)||09/14/16|
|2016||Biorefinery lignosulfonates from sulfite-pretreated softwoods as dispersant for graphite||12/02/16|
|2016||Chapter 7: Use of VFM for Heterogeneity Evaluation of Materials Under Uniaxial Tensile Stress||01/07/16|
|2016||Chapter 8 optimized test design for identification of the variation of elastic stiffness properties of Loblolly Pine (Pinus taeda) pith to bark||11/02/16|
|2016||Conversion of SPORL pretreated Douglas fir forest residues into microbial lipids with oleaginous yeasts||05/03/16|
|2016||Efficient Conversion of Lignin to Electricity Using a Novel Direct Biomass Fuel Cell Mediated by Polyoxomethalates at Low Temperatures||05/04/16|
|2016||Endoglucanase post-milling treatment for producing cellulose nanofibers from bleached eucalyptus fibers by a supermasscolloider||07/15/16|
|2016||Fabrication of microfibrillated cellulose gel from waste pulp sludge via mild maceration combined with mechanical shearing||12/02/16|
|2016||Fermentative high-titer ethanol production from Douglas-fir forest residue without detoxification using SPORL: high SO2 loading at low temperature||10/05/17|
|2016||Green and low-cost production of thermally stable and carboxylated cellulose Nanocrystals and nanofibrils using highly recyclable dicarboxylic acids||03/01/17|
|2016||Highly thermal-stable and functional cellulose nanocrystals and nanofibrils produced using fully recyclable organic acids||07/15/16|
|2016||Highly transparent, low-haze, hybrid cellulose nanopaper as electrodes for flexible electronics||12/06/16|
|2016||Microbial lipid production from SPORL-pretreated Douglas fir by Mortierella isabellina||05/03/16|
|2016||Molecular structure of sodium lignosulfonate from different sources and their properties as dispersant of TiO2 slurry||12/20/16|
|2016||Pilot-scale demonstration of SPORL for bioconversion of lodgepole pine to bioethanol and lignosulfonate||07/28/16|
|2016||Probing crystallinity of never-dried wood cellulose with Raman spectroscopy||01/07/16|
|2016||Techniques for characterizing lignin||09/22/16|
|2016||Understanding longitudinal wood fiber ultra-structure for producing cellulose nanofibrils using disk milling with diluted acid prehydrolysis||02/10/17|
|2016||Wood-derived materials for green electronics, biological Devices, and energy applications||12/20/16|
|2015||Case studies on sugar production from underutilized woody biomass using sulfite chemistry||10/15/15|
|2015||Cellulose Nanocrystal Entrapment of Benzalkonium Chloride in Southern Pine: Biological, Chemical, and Physical Properties||09/15/15|
|2015||Comparison of Cellulose Supramolecular Structures Between Nanocrystals of Different Origins||09/25/15|
|2015||Effect of Hot-Pressing Temperature on the Subsequent Enzymatic Saccharification and Fermentation Performance of SPORL Pretreated Forest Biomass||04/01/15|
|2015||Effects of process variables on the yield stress of rheologically modified biomass||09/29/16|
|2015||Estimation of S/G ratio in woods using 1064 nm FT-Raman spectroscopy||09/25/15|
|2015||Facile preparation of nanofiller-paper using mixed office paper without deinking||04/30/15|
|2015||Formation of Irreversible H-bonds in Cellulose Materials||09/25/15|
|2015||High titer and yield ethanol production from undetoxified whole slurry of Douglas-fir forest residue using pH profiling in SPORL||04/30/15|
|2015||High Titer Ethanol and Lignosulfonate Production from SPORL Pretreated Poplar at Pilot Scale||09/25/15|
|2015||Highly transparent and toughened poly(methyl methacrylate) nanocomposite films containing networks of cellulose nanofibrils||09/28/16|
|2015||LCA Study for Pilot Scale Production of Cellulose Nano Crystals (CNC) from Wood Pulp||04/28/16|
|2015||Mountain pine beetle infestation: GCxGCTOFMS and GC-MS of lodgepole pine (pinus contorta) acetone extractives||05/19/16|
|2015||Naturally p-Hydroxybenzoylated Lignins in Palms||09/15/15|
|2015||New Model of Wood Cell Wall Microfibril and Its Implications||09/25/15|
|2015||Optimizing cellulose fibrillation for the production of cellulose nanofibrils by a disk grinder||10/07/15|
|2015||Physical and Mechanical Properties of Cellulose Nanofibril Films from Bleached Eucalyptus Pulp by Endoglucanase Treatment and Microfluidization||09/25/15|
|2015||Production of cellulose nanofibrils from bleached eucalyptus fibers by hyperthermostable endoglucanase treatment and subsequent microfluidization||02/11/15|
|2015||Regulation of Gene Expression during the Onset of Ligninolytic Oxidation by Phanerochaete chrysosporium on Spruce Wood||12/15/15|
|2015||Self-assembled optically transparent cellulose nanofibril films: effect of nanofibril morphology and drying procedure||04/01/15|
|2015||Tailoring the yield and characteristics of wood cellulose nanocrystals (CNC) using concentrated acid hydrolysis||09/25/15|
|2015||The effect of polarity of extractives on the durability of wood||05/19/16|
|2015||Using a combined hydrolysis factor to optimize high titer ethanol production from sulfite-pretreated poplar without detoxification||04/08/15|
|2015||Using sulfite chemistry for robust bioconversion of Douglas-fir forest residue to bioethanol at high titer and lignosulfonate: A pilot-scale evaluation||01/21/15|
|2014||1064nm FT-Raman spectroscopy for investigations of plant cell walls and other biomass materials||09/25/14|
|2014||A Highly Diastereoselective Oxidant Contributes to Ligninolysis by the White Rot Basidiomycete Ceriporiopsis subvermispora||10/01/14|
|2014||A novel rheometer design for yield stress fluids||09/30/14|
|2014||Alkaline Method for Dissolving Cellulose *||09/22/14|
|2014||Characterization of cellulose nanofibrillation by micro grinding||07/21/14|
|2014||Characterization of Paper Heterogeneity||08/14/14|
|2014||Comparison between Cellulose Nanocrystal and Cellulose Nanofibril Reinforced Poly(ethylene oxide) Nanofibers and Their Novel Shish-Kebab-Like Crystalline Structures||07/21/14|
|2014||Comparison of Dilute Acid and Sulfite Pretreatment for enzymatic Saccharification of Earlywood and Latewood of Douglas Fir||03/28/14|
|2014||Comparisons of five Saccharomyces cerevisiae strains for ethanol production from SPORL pretreated lodgepole pine||12/23/14|
|2014||Comparisons of high titer ethanol production and lignosulfonate properties by SPORL pretreatment of lodgepole pine at two temperatures||08/07/14|
|2014||Delignification of Wood Pulp by Vanadium-Substitute Polyoxometalates *||09/23/14|
|Below are 13 research projects associated with this research unit.|
|Project Number||Title||Project Dates|
|FPL-4709-2B||Advancement of the Science and use of Cellulose Nano-Materials||10-01-2012 - 09-30-2017|
|FPL-4709-1A||Advancing the forest biorefinery||08-24-2007 - 08-23-2012|
|FPL-4709-3-T||Developing new and innovative methods to convert wood and other lignocellulosics into fibers and chemicals||07-31-2002 - 07-30-2007|
|FPL-4709-2A||Development of cellulose nano-crystals||08-24-2007 - 08-23-2012|
|FPL-4709-2-T||Improved papermaking properties of high-yield mechanical and chemi-mechanical pulps, which make more efficient use of our wood resource||07-31-2002 - 07-30-2007|
|FPL-4709-1-T||New technologies for the fractionation of wood to produce pulp and to bleach it||07-31-2002 - 07-30-2007|
|FPL-4709-4B||Paper and Fiber Physics||10-01-2012 - 09-30-2017|
|FPL-4709-4A||Recycle and deinking of waste paper||08-24-2007 - 08-23-2012|
|FPL-4709-5A||Strength and performance of paper and paperboard||08-24-2007 - 08-23-2012|
|FPL-4709-1B||The Forest Biorefinery||10-01-2012 - 09-30-2017|
|FPL-4709-4-T||Understand the biogenesis and molecular architecture of wood cell walls, environmental stresses and transformation in the industrial process||07-31-2002 - 07-30-2007|
|FPL-4709-3B||Wood Fiber and Chemical Products||10-01-2012 - 09-30-2017|
|FPL-4709-3A||Wood fiber and pulping||08-24-2007 - 08-23-2012|
|Forest Thinnings Produce Thermomechanical Pulp and Quality Lumber|
A research collaboration among FPL, University of Idaho (Moscow), Pacific Northwest Research Station, Colville National Forest, Ponderay Newsprint Company (PNC), and Ponderay Valley Fiber (PVF) has addressed two forestry-related issues, one of environmental and one of economic concern: overcrowding of forests in the western United States and a diminishing supply of pulpwood from public and private lands in the same region.
Preliminary FPL research showed that small-diameter, thinned trees, once thought to be inferior, are in fact suitable for lumber and pulp production. Furthermore, less refining energy was required to produce pulp from forest thinnings than from conventional wood supplies. To convince the pulp and paper industry that thinnings are a good alternative source of wood fiber, researchers demonstrated their findings at Ponderay Newsprint company and Ponderay Valley Fiber. Results of this study show that lumber produced from forest thinnings meets or exceeds the saw mill specification. Chips generated from forest thinnings as either whole logs or sawmill residuals produced commercial-quality thermomechanical pulp for newsprint.
This collaboration with the Pacific Northwest Research Station and Colville National Forest continues, now evaluating bark-beetle-killed pines for use in pulping and paper products.
Below are the 10 most recent Lab Notes blog postings pertaining to this research unit.
|FPL Research Helps Fuel Coast-to-Coast Flight|
Washington state-based Alaska Airlines made history flying the first commercial flight using the world’s first renewable, alternative jet fuel. The fuel was made from forest residuals, the limbs and branches that remain after the harvesting of mana...
|FPL Partner Procures Patent:|
Whether serving as a bookshelf, tabletop, or wall panel, the composite board is a ubiquitous construction material found in furniture and homes alike. Traditional composite boards use mankind's most trusted building resource, wood, as a base — but ...
|Researchers Honored with Fellowship|
TAPPI, the leading association for the worldwide pulp, paper, packaging, and converting industries, has announced the selection of FPL’s Carl Houtman and Junyong Zhu as TAPPI Fellows...
|FPL Researcher Receives 2014 TAPPI Research and Development Technical Award|
JunYong Zhu, research general engineer at the Forest Products Laboratory, is winner of the 2014 Research and Development Technical Award and William H. Aiken Prize by TAPPI’s International Research Management Committee (IRMC). This award is given f...
|A Winning Paper...on Paper|
A journal article authored by Forest Products Laboratory researchers David Vahey (retired) and John Considine has been selected as the TAPPI Journal Best Research Paper for 2013...
|Women's History Month: FPL Remembers Marguerite Sykes|
Is paper one of the first things that comes to mind when you think about forest products? FPL has been at the forefront of developing innovative and environmentally friendly methods for producing this ubiquitous product. Chemist Marguerite Sykes, wh...
|Distinguished Scientist Award Goes to FPL Researcher|
JunYong Zhu, research general engineer at the Forest Products Laboratory, was recently presented with the Forest Service Deputy Chief's Distinguished Science Award...
This image from the 1980's shows Forest Products Laboratory (FPL) employee Vance Setterholm standing at the reel end of the paper machine in FPL's pilot plant. He's inspecting a corrugated container made from press-dried paper...
|A "Nexus of Innovation" for the U.S. Forest Service|
In a recent feature story from xconomy.com, FPL Director Michael Rains describes the Forest Products Laboratory as "a one-of-a-kind resource at the intersection of many Forest Service goals."
|Hydrogen peroxide and caustic soda:|
When hydrogen peroxide is mixed with caustic soda as part of the pulping or paper-making process, potentially dangerous amounts of heat and oxygen can develop. As a result, catastrophic events have occurred at several mills in Europe and North Americ...