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Forest Products Laboratory
One Gifford Pinchot Drive
Madison, WI 53726-2398
Phone: (608) 231-9200
Fax: (608) 231-9592
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Forest Biopolymer Science and Engineering

Project Title :  Developing advanced materials through property enhancement at nano- and micro- dimensions
Project Number : FPL-4707-3A
Status : TERMINATED
Start Date : 08-24-2007
End Date : 08-23-2012


View the 38 publications associated with this project.

Gregory SchuenemanPrincipal Investigator:
Gregory Schueneman

Non Technical Summary
The nanotechnologies and nano-materials developed at FPL under this problem have a high probability for success and for use by industry. The expected gains of the research will be to improve existing products and processes. Nanotechnology and processing techniques will enable industry to develop wood products that are more competitive with other building products. Products include new wood-based products having improved dimensional stability, adhesive qualities, fire, decay, and termite resistance with treatments that are environmentally safe to produce, use, and dispose of. Nanotechnology will aid in the conversion of low value forest residues, fire and insect destroyed stands to value-added forest materials and feedstocks.


Objectives Summary
Using nanotechnology concept and methods, researchers will investigate the intrinsic properties of lignocellulosic materials and the influence of modifications of wood polymer components at the molecular, nano, and cell wall dimensions. With this in mind, there are five focus areas that need to be developed. 1) Develop fundamental knowledge of nano-scale phenomena and processes and elucidate scientific and engineering principles and mechanisms governing these phenomena and processes. 2) Develop comprehensive understanding of how changes at the nano-scale modify the physical, chemical, and biological properties at the micro and macroscopic dimensions. 3) Develop new generation of instruments to measure materials properties at the nano-scale. 4) Develop methods for synthesis, structure evaluation, materials and systems design. 5) Develop standards for testing, manufacture, and characterization of nano-materials.


Approach Summary
Investigating lignocellulosic materials at the nano-scale requires a comprehensive assessment in the types of analysis techniques that will be necessary to measure the desired property, feature, characteristic, or interaction. The use of conventional or established testing techniques and equipment will continue to be central to our research efforts; however, new testing techniques need to be developed so that lignocellulosic materials can be evaluated in innovative ways, thus providing a new perspective in the characterization of lignocellulosic materials. Likewise, it will be necessary to develop new equipment or modify equipment on the basis of advances in nanotechnology from other industries. There will be four focus areas for technique & equipment development: Nano-scale sensors, Nano-scale processing and process control, Analytical methods for nanostructure characterization, and Dissolution techniques.

Publications associated with this Project

Publication YearTitleDate Posted
2010Analysis of indentation creep05/17/10
2011Applications of nanoindentation-based mechanical spectroscopy in forest products research (abstract)10/06/11
2010Atomic Force Microscopy Characterization of Cellulose Nanocrystals05/17/10
2012Broadband nanoindentation of glassy polymers: Part I Viscoelasticity03/26/12
2012Broadband nanoindentation of glassy polymers: Part II. Viscoplasticity03/26/12
2011Calculation of single chain cellulose elasticity using fully atomistic modeling06/06/11
2011Cellulose nanomaterials review: structure, properties and nanocomposites07/12/11
2008Characterization of Cellulose Nanocrystal Surfaces by SPM11/20/09
2010Characterizing Polymeric Methylene Diphenyl Diisocyanate Reactions with Wood: 1. High-Resolution Solution-State NMR Spectroscopy11/26/10
2010Characterizing Polymeric Methylene Diphenyl Diisocyanate Reactions with Wood: 2. Nano-Indentation11/26/10
2009Creep properties of micron-size domains in ethylene glycol modified wood across 4½ decades in strain rate07/06/09
2011Delineating pMDI model reactions with loblolly pine via solution state NMR spectroscopy. Part2.Non-catalyzed reactions with the wood cell wall03/29/11
2011Delineating pMDI model reactions with loblolly pine via solution-state NMR spectroscopy. Part 1. Catalyzed reations with wood models and wood polymers03/29/11
2011Development of the metrology and imaging of celllulose nanocrystals03/21/11
2010Elastic Deformation Mechanics of Cellulose Nanocrystals05/17/10
2010Evaluation Of Adhesive Penetration Of Wood Fibre By Nanoindentation And Microscopy11/26/10
2012Examination of water phase transitions in Loblolly pine and cell wall components by differential scanning calorimetry04/19/12
2009Investigation of thermally activated deformation in amorphous PMMA and Zr-Cu-Al bulk metallic glasses with broadband nanoindentation creep04/27/09
2012Lignin-Based Electrospun Nanofibers Reinforced with Cellulose Nanocrystals09/17/12
2011Litter decay rates are determined by lignin chemistry10/23/11
2012Modeling hygroelastic properties of genetically modified aspen01/27/12
2011Multidimensional NMR analysis reveals truncated lignin structures in wood decayed by the brown rot basidiomycete Postia placenta10/23/11
2011Multidimensional NMR analysis reveals truncated lignin structures in wood decayed by the brown rot basidiomycete Postia placenta11/07/11
2009Nanoindentation near the edge04/27/09
2007Nanoindentation of the interphase region of a wood-reinforced polypropylene composite10/15/10
2011Nanomechanical study of amorphous and polycrystalline ALD HfO2 thin films09/29/11
2011Nanoreinforced biocompatible hydrogels from wood hemicelluloses and cellulose whiskers10/23/11
2012Polymer Matrix Nanocomposites via Forest Derived Nanomaterials09/18/12
2009Relating Nanoindentation to Macroindentation of Wood02/09/10
2012Research into Cellulose nanomaterials spans the globe07/03/12
2011Self-assembly and alignment of semiconductor nanoparticles on cellulose nanocrystals07/12/11
2012Semi-Interpenetrating polymer network hydrogels based on aspen hemicellulose and chitosan: Effect of crosslinking sequence on hydrogel properties09/27/12
2009Shear Transformation Zone Activation During Deformation in Bulk Metallic Glasses Characterized Using a New Indentation Creep Technique02/09/10
2011The edge effect in nanoindentation05/16/11
2009Tools for the Characterization of Biomass at the Nanometer Scale10/06/09
2011Tools to Understand Structural Property Relationships for Wood Cell Walls09/27/12
2010Transverse Elasticity of Cellulose Nanocrystals Via Atomic Force Microscopy05/17/10
2011Uncertainty quantification in nanomechanical measurements using the atomic force microscope07/03/12

Project Summaries last modified: 06-22-2011