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Title: A novel sample preparation method to avoid influence of embedding medium during nano-indentation

Source: Appl Phys A, Published online: 25 August 2012.

Author(s)Meng, Yujie; Wang, Siqun; Cai, Zhiyong; Young, Timothy M.; Du, Guanben; Li, Yanjun

Publication Year: 2012  View PDF »

Category: Journal Articles
Associated Research Project(s):   FPL-4706-1A

Abstract: The effect of the embedding medium on the nano-indentation measurements of lignocellulosic materials was investigated experimentally using nano-indentation. Both the reduced elastic modulus and the hardness of nonembedded cell walls were found to be lower than those of the embedded samples, proving that the embedding medium used for specimen preparation on cellulosic material during nano-indentation can modify cell-wall properties. This leads to structural and chemical changes in the cell-wall constituents, changes that may significantly alter the material properties. Further investigation was carried out to detect the influence of different vacuum times on the cell-wall mechanical properties during the embedding procedure. Interpretation of the statistical analysis revealed no linear relationships between vacuum time and the mechanical properties of cell walls. The quantitative measurements confirm that low-viscosity resin has a rapid penetration rate early in the curing process. Finally, a novel sample preparation method aimed at preventing resin diffusion into lignocellulosic cell walls was developed using a plastic film to wrap the sample before embedding. This method proved to be accessible and straightforward for many kinds of lignocellulosic material, but is especially suitable for small, soft samples.

Keywords: nano-indentation measurements, lignocellulosic materials, embedding medium

Publication Review Process: Formally Refereed

File size: 1,061 kb(s)

Date posted: 10/05/2012

This publication is also viewable on Treesearch:  view
RITS Product ID: 62392
Current FPL Scientist associated with this product
Cai, Zhiyong
Supervisory Research Materials Engineer

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